(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

Base Information

Chemical Name:(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide
CAS No.:161283-41-6
Molecular Formula:C₂₀H₂₉N₃O₃
Molecular Weight:359.469
Hs Code.:

Synonyms:(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

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Technology Process of (S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

There total 5 articles about (S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-1-((Z)-2-Benzoylamino-4,4-dimethyl-pent-2-enoyl)-pyrrolidine-2-carboxylic acid methylamide

: (S)-1-((S)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

: 161283-41-6
(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In toluene; at 50 ℃; for 48h; Yield given. Yields of byproduct given;
DOI:10.1039/c39940001915

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 161283-41-6
(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Pb(OAc)2, Ac₂O / 72 h / Heating

2: 74 percent / CHCl₃ / 1) 0 deg C to 20 deg C, 14 h, 2) 50 deg C, 1 h

3: H₂ / Pd/C / toluene / 48 h / 50 °C

With hydrogen; lead acetate; acetic anhydride; palladium on activated charcoal; In chloroform; toluene;
DOI:10.1039/c39940001915

Reference yield:

: 52060-82-9
L-proline methylamide

: 161283-41-6
(S)-1-((R)-2-Benzoylamino-4,4-dimethyl-pentanoyl)-pyrrolidine-2-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / CHCl₃ / 1) 0 deg C to 20 deg C, 14 h, 2) 50 deg C, 1 h

2: H₂ / Pd/C / toluene / 48 h / 50 °C

With hydrogen; palladium on activated charcoal; In chloroform; toluene;
DOI:10.1039/c39940001915