1.4-disodium-1.1.4.4-tetraphenylic butane

Base Information

• Chemical Name: 1.4-disodium-1.1.4.4-tetraphenylic butane
• CAS No.: 26232-99-5
• Molecular Formula: C₂₈H₂₄*2Na
• Molecular Weight: 406.478
• Mol file: 26232-99-5.mol

Synonyms:1.4-disodium-1.1.4.4-tetraphenylic butane

Chemical Property of 1.4-disodium-1.1.4.4-tetraphenylic butane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1.4-disodium-1.1.4.4-tetraphenylic butane

There total 1 articles about 1.4-disodium-1.1.4.4-tetraphenylic butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1.4-disodium-1.1.4.4-tetraphenylic butane (26232-99-5)

Guidance literature:

1,1-Diphenyl-aethylen, NaI, elektrolyt. Red., Hexamethylphosphorsaeuretriamid (nicht isoliert, nach Hydrolyse als 1,1,4,4-Tetraphenyl-butan nachgewiesen);

DOI:10.1016/S0022-328X(00)88045-6

Reference yield:

triphenylborane (960-71-4) + 1.4-disodium-1.1.4.4-tetraphenylic butane (26232-99-5) → sodium triphenyl boronhydride (63706-82-1) + 1,1,4,4-tetraphenyl-1,3-butadiene (1450-63-1)

Guidance literature:

In diethyl ether; molar ratio of B(C6H5)3:(C6H5)2CNaCH2CH2CNa(C6H5)2=2:1;

Reference yield:

1.4-disodium-1.1.4.4-tetraphenylic butane (26232-99-5) → triphenylborane (960-71-4)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: mineral acid / not given

With mineral acid; In diethyl ether;

Downstream raw materials:

sodium triphenyl boronhydride

1,1,4,4-tetraphenyl-1,3-butadiene

triphenylborane