3-(2-carboxybenzylthio)phenyl acetic acid

Base Information

Chemical Name:3-(2-carboxybenzylthio)phenyl acetic acid
CAS No.:83794-93-8
Molecular Formula:C₁₆H₁₄O₄S
Molecular Weight:302.351
Hs Code.:

Synonyms:3-(2-carboxybenzylthio)phenyl acetic acid

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Chemical Property of 3-(2-carboxybenzylthio)phenyl acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 3-(2-carboxybenzylthio)phenyl acetic acid

There total 11 articles about 3-(2-carboxybenzylthio)phenyl acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 83794-92-7
3-(2-carboxybenzylthio)phenylacetonitrile

: 83794-93-8
3-(2-carboxybenzylthio)phenyl acetic acid

Guidance literature:: With phosphoric acid; In acetic acid; for 7h; Heating;

Reference yield: 90.0%

: 83794-91-6
3-(2-carboxymethylbenzylthio)phenylacetonitrile

: 83794-93-8
3-(2-carboxybenzylthio)phenyl acetic acid

Guidance literature:: With sulfuric acid; In methanol; water; for 23h; Heating;

Reference yield:

: 4025-64-3
3-Carboxybenzenesulfonyl chloride

: 83794-93-8
3-(2-carboxybenzylthio)phenyl acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminum hydride / tetrahydrofuran / 1 h

2: dimethylformamide; H₂O / 0.33 h / Ambient temperature

3: 78.4 percent / sodium hydroxide; HCl / methanol; H₂O / 1 h / Heating

4: 92 percent / dry hydrogen bromide / tetrahydrothiophene 1,1-dioxide / 3 h / 15 °C

5: sodium hydroxide / methanol; H₂O / 1 h / Heating

6: 90 percent / 85percent phosphoric acid / acetic acid / 7 h / Heating

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; phosphoric acid; hydrogen bromide; In tetrahydrofuran; sulfolane; methanol; water; acetic acid; N,N-dimethyl-formamide;