Technology Process of C26H22N2O5
There total 4 articles about C26H22N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; potassium carbonate;
In
1,4-dioxane;
at 100 ℃;
for 15h;
Inert atmosphere;
DOI:10.1039/c2ob26267c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydroxylamine hydrochloride; sodium hydroxide / water; ethanol / 2 h / Cooling with ice
2: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
3: triethylamine / toluene / 19 h / 80 °C
4: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; potassium carbonate / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere
With
N-chloro-succinimide; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; hydroxylamine hydrochloride; potassium carbonate; triethylamine; sodium hydroxide;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2ob26267c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / toluene / 19 h / 80 °C
2: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; potassium carbonate / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere
With
[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; potassium carbonate; triethylamine;
In
1,4-dioxane; toluene;
DOI:10.1039/c2ob26267c
