3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

Base Information

Chemical Name:3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole
CAS No.:1360555-00-5
Molecular Formula:C₂₃H₁₄ClF₃N₄
Molecular Weight:438.839
Hs Code.:

Synonyms:3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

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Technology Process of 3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

There total 5 articles about 3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1360554-90-0
2-(azidobenzylideneamino)-1-(4-chlorophenyl)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1

: 1360555-00-5
3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

Guidance literature:: With triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 4h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201100710

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 1360555-00-5
3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine; acetic acid

2: ethanol / 3 h / 20 °C

3: ethanol / 50 °C

4: triphenylphosphine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With piperidine; acetic acid; triphenylphosphine; In ethanol; dichloromethane; 3: Aza-Wittig reaction;
DOI:10.1002/ejoc.201100710

Reference yield:

: 1360555-43-6
C₁₆H₉ClF₃N₃O

: 1360555-00-5
3-(4-chlorophenyl)-2-[4-(trifluoromethyl)benzyl]-1,2,4-triazino-[2,3-b]indazole

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3 h / 20 °C

2: ethanol / 50 °C

3: triphenylphosphine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With triphenylphosphine; In ethanol; dichloromethane; 2: Aza-Wittig reaction;
DOI:10.1002/ejoc.201100710