N-(4-nitrobenzyl)-N’-phenylurea

Base Information

Chemical Name:N-(4-nitrobenzyl)-N’-phenylurea
CAS No.:1366179-97-6
Molecular Formula:C₁₄H₁₃N₃O₃
Molecular Weight:271.276
Hs Code.:

Synonyms:N-(4-nitrobenzyl)-N’-phenylurea

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Chemical Property of N-(4-nitrobenzyl)-N’-phenylurea

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Technology Process of N-(4-nitrobenzyl)-N’-phenylurea

There total 4 articles about N-(4-nitrobenzyl)-N’-phenylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 619-73-8
4-nitrobenzyl chloride

: 622-34-4
1-phenylcyanamide

: 1366179-97-6
N-(4-nitrobenzyl)-N’-phenylurea

Guidance literature:: With iron(III) chloride; In 1,2-dichloro-ethane; for 7h; Reflux;
DOI:10.1039/c2ob06916d

Reference yield: 75.0%

: 2594-09-4
N-hydroxy-2-(4-nitrophenyl)acetamide

: 62-53-3
aniline

: 1366179-97-6
N-(4-nitrobenzyl)-N’-phenylurea

Guidance literature:: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; carbon tetrabromide; N,N-dimethyl-formamide; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere; Irradiation; Green chemistry;
DOI:10.1039/c4ra03805c

Reference yield:

: 62-53-3
aniline

: 1366179-97-6
N-(4-nitrobenzyl)-N’-phenylurea

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 0 °C

2: iron(III) chloride / 1,2-dichloro-ethane / 7 h / Reflux

With iron(III) chloride; triethylamine; In diethyl ether; 1,2-dichloro-ethane; 2: Ritter reaction;
DOI:10.1039/c2ob06916d