1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien

Base Information

• Chemical Name: 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien
• CAS No.: 121968-19-2
• Molecular Formula: C₃₁H₂₄N₆
• Molecular Weight: 480.572

Synonyms:1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien

Chemical Property of 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien

Chemical Property:

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Technology Process of 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien

There total 1 articles about 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene (2267-32-5) + aniline yellow (60-09-3) → 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien (121968-19-2)

Guidance literature:

With triethylamine;

DOI:10.1021/ja01475a031

Reference yield:

tetracarbonyl nickel (13463-39-3,71564-36-8) + 1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien (121968-19-2) → {Ni(C6H5NNC6H4NC7H5NC6H4NNC6H5)2} (108486-52-8)

Guidance literature:

In methanol; boiling methanol;

DOI:10.1021/ja01475a031

Reference yield:

1-(p-Benzolazo-phenylamino)-7-(p-benzolazo-phenylimino)-cyclohepta-1,3,5-trien (121968-19-2) + nickel dichloride (83864-14-6) → {Ni(C6H5NNC6H4NC7H5NC6H4NNC6H5)2} (108486-52-8)

Guidance literature:

With sodium acetate; In ethanol; dichloromethane; water; boiling soln.;

DOI:10.1021/ja01475a031

upstream raw materials:

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene

aniline yellow

Downstream raw materials:

{Ni(C₆H₅NNC₆H₄NC₇H₅NC₆H₄NNC₆H₅)2}

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