Technology Process of methyl 2-(2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate
There total 6 articles about methyl 2-(2-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane;
for 18h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; potassium hydroxide / ethanol / 2 h / Reflux
2: thionyl chloride / 4 h / 0 °C / Reflux
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 18 h / Reflux; Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; thionyl chloride; water; potassium acetate; potassium hydroxide;
In
ethanol; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C
2: thionyl chloride / dichloromethane / 4 h / 0 °C / Reflux
3: ethanol / 12 h / Reflux
4: water; potassium hydroxide / ethanol / 2 h / Reflux
5: thionyl chloride / 4 h / 0 °C / Reflux
6: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 18 h / Reflux; Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; thionyl chloride; water; potassium acetate; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;
