N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

Base Information

Chemical Name:N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide
CAS No.:1627523-03-8
Molecular Formula:C₁₇H₁₆N₄O₃
Molecular Weight:324.339
Hs Code.:

Synonyms:N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

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Chemical Property of N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

Chemical Property:

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Technology Process of N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

There total 8 articles about N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1627522-94-4
7-amino-3-((4-methoxyphenyl)amino)quinoxalin-2(1H)-one

: 75-36-5
acetyl chloride

: 1627523-03-8
N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

Guidance literature:: In tetrahydrofuran; for 24h; Reflux;
DOI:10.1016/j.bioorg.2014.05.010

Reference yield:

: 1627522-93-3
3-((4-methoxyphenyl)amino)-7-nitroquinoxalin-2(1H)-one

: 1627523-03-8
N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C

2: tetrahydrofuran / 24 h / Reflux

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;
DOI:10.1016/j.bioorg.2014.05.010

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1627523-03-8
N-(2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / water / 2 h / Reflux

2: potassium nitrate; sulfuric acid / 20 °C

3: trichlorophosphate / 6 h / Reflux

4: isopropyl alcohol / 20 °C

5: hydrogenchloride / water / 50 °C

6: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C

7: tetrahydrofuran / 24 h / Reflux

With hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium nitrate; trichlorophosphate; In tetrahydrofuran; methanol; water; isopropyl alcohol;
DOI:10.1016/j.bioorg.2014.05.010