2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

Base Information

Chemical Name:2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one
CAS No.:1308253-48-6
Molecular Formula:C₁₆H₁₇N₃O₂S
Molecular Weight:315.396
Hs Code.:

Synonyms:2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

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Chemical Property of 2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

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Technology Process of 2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

There total 3 articles about 2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5950-19-6
3-chloro-3-methyl-2-butanone

: C₁₁H₁₁N₃O₂S

: 1308253-48-6
2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

Guidance literature:: 3-chloro-3-methyl-2-butanone; C₁₁H₁₁N₃O₂S; In ethanol; water; for 0.25h; Reflux;

With sodium acetate; In ethanol; water; at 0 ℃; Reflux;
DOI:10.1016/j.tet.2011.03.011

Reference yield:

: 2-(benzylthio)-6-hydroxy-5-nitroso-pyrimidin-4(3H)-one

: 1308253-48-6
2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dithionite / ethanol; water / 20 °C / Darkness

2.1: ethanol; water / 0.25 h / Reflux

2.2: 0 °C / Reflux

With sodium dithionite; In ethanol; water;
DOI:10.1016/j.tet.2011.03.011

Reference yield:

: 148020-95-5
C₁₁H₁₀N₂O₂S

: 1308253-48-6
2-(benzylsulfanyl)-6,7,7-trimethyl-3,7-dihydro-4H-pyrimido[4,5-b][1,4]oxazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: cis-nitrous acid

2.1: sodium dithionite / ethanol; water / 20 °C / Darkness

3.1: ethanol; water / 0.25 h / Reflux

3.2: 0 °C / Reflux

With sodium dithionite; cis-nitrous acid; In ethanol; water;
DOI:10.1016/j.tet.2011.03.011