(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

Base Information

Chemical Name:(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide
CAS No.:116407-98-8
Molecular Formula:C₂₁H₂₆NO₅P
Molecular Weight:403.415
Hs Code.:

(4R,6R)-2-<(1S)-2-phenyl-1-<N-(phenylmethoxycarbonyl)amino>ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

Synonyms:(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

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Chemical Property of (4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

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Technology Process of (4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

There total 4 articles about (4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 42075-32-1
(2R,4R)-pentanediol

: 116381-45-4
C₁₆H₁₆Cl₂NO₃P

: 116407-98-8
(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

Guidance literature:: With triethylamine; In dichloromethane; for 1h;

Reference yield:

: 66609-42-5
D-Phenylalanine phosphonate

: 116407-98-8
(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaHCO₃, Na₂CO₃, 2 N NaOH / 20 h / 21 °C

2: SOCl₂ / CH₂Cl₂ / 4 h / 21 °C

3: 95 percent / Et₃N / CH₂Cl₂ / 1 h

With sodium hydroxide; thionyl chloride; sodium hydrogencarbonate; sodium carbonate; triethylamine; In dichloromethane;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 116407-98-8
(4R,6R)-2-<(1S)-2-phenyl-1-ethyl>-4,6-dimethyl-1,3,2-dioxaphosphorinane-2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaHCO₃, Na₂CO₃, 2 N NaOH / 20 h / 21 °C

2: SOCl₂ / CH₂Cl₂ / 4 h / 21 °C

3: 95 percent / Et₃N / CH₂Cl₂ / 1 h

With sodium hydroxide; thionyl chloride; sodium hydrogencarbonate; sodium carbonate; triethylamine; In dichloromethane;