(1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

Base Information

• Chemical Name: (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione
• CAS No.: 49593-11-5
• Molecular Formula: C₁₇H₂₂N₂O₄S₂
• Molecular Weight: 382.505

Synonyms:(1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

Chemical Property of (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

There total 3 articles about (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3r,6t-dimercapto-1,4-dimethyl-piperazine-2,5-dione (49593-00-2) → (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione (49593-11-5)

Guidance literature:

Multi-step reaction with 3 steps

1: BF₃-Et₂O / CH₂Cl₂

2: (i) nBuLi, THF, (ii) /BRN= 969135/

3: (i) nBuLi, THF, (ii) /BRN= 969135/

With boron trifluoride diethyl etherate; In dichloromethane;

DOI:10.1021/ja00800a077

Reference yield:

3r,6c-dimercapto-1,4-dimethyl-piperazine-2,5-dione (19552-98-8,33045-33-9,49593-00-2) → (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione (49593-11-5)

Guidance literature:

Multi-step reaction with 3 steps

1: BF₃-Et₂O / CH₂Cl₂

2: (i) nBuLi, THF, (ii) /BRN= 969135/

3: (i) nBuLi, THF, (ii) /BRN= 969135/

With boron trifluoride diethyl etherate; In dichloromethane;

DOI:10.1021/ja00800a077

Reference yield:

3-(4-methoxy-phenyl)-1,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione (49593-08-0) + methyl iodide (74-88-4) → (1R,3R,5R)-1-Methoxymethyl-3-(4-methoxy-phenyl)-5,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione (49593-11-5)

Guidance literature:

Multistep reaction; (i) nBuLi, THF, (ii) /BRN= 969135/;

DOI:10.1021/ja00800a077

upstream raw materials:

3-(4-methoxy-phenyl)-1,6,8-trimethyl-2,4-dithia-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

methyl iodide

3r,6t-dimercapto-1,4-dimethyl-piperazine-2,5-dione

3r,6c-dimercapto-1,4-dimethyl-piperazine-2,5-dione

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