(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

Base Information

Chemical Name:(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine
CAS No.:1416070-04-6
Molecular Formula:C₂₆H₂₇N₃O₄
Molecular Weight:445.518
Hs Code.:

Synonyms:(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

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Chemical Property of (3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

Chemical Property:

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Technology Process of (3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

There total 3 articles about (3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416070-03-5
tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

: 1416070-04-6
(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

Reference yield:

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 1416070-04-6
(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

1.2: 2 h

2.1: hydroxylamine / ethanol; water / 16 h / 80 °C

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C

3.2: 0.5 h / 150 °C / microwave irradiation

4.1: hydrogenchloride / 1,4-dioxane; methanol / 2 h / 20 °C

With hydrogenchloride; hydroxylamine; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 4-(1,3-dioxolan-2-ylmethyl)benzonitrile

: 1416070-04-6
(3-((3-(4-(2,2-dimethoxyethyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine / ethanol; water / 16 h / 80 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C

2.2: 0.5 h / 150 °C / microwave irradiation

3.1: hydrogenchloride / 1,4-dioxane; methanol / 2 h / 20 °C

With hydrogenchloride; hydroxylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; ethanol; water; acetonitrile;