tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

Base Information

Chemical Name:tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate
CAS No.:1416070-03-5
Molecular Formula:C₃₁H₃₃N₃O₆
Molecular Weight:543.62
Hs Code.:

Synonyms:tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

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Chemical Property of tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

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Technology Process of tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

There total 3 articles about tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416070-02-4
4-((1,3-dioxolan-2-yl)methyl)-N'-hydroxybenzimidamide

: 1416069-85-6
2-(3-(((tert-butoxycarbonyl)amino)(phenyl)methyl)phenoxy)acetic acid

: 1416070-03-5
tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

Guidance literature:: 4-((1,3-dioxolan-2-yl)methyl)-N'-hydroxybenzimidamide; 2-(3-(((tert-butoxycarbonyl)amino)(phenyl)methyl)phenoxy)acetic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 16h;

With pyridine; In acetonitrile; at 150 ℃; for 0.5h; microwave irradiation;

Reference yield:

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 1416070-03-5
tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

1.2: 2 h

2.1: hydroxylamine / ethanol; water / 16 h / 80 °C

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C

3.2: 0.5 h / 150 °C / microwave irradiation

With hydroxylamine; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 4-(1,3-dioxolan-2-ylmethyl)benzonitrile

: 1416070-03-5
tert-butyl ((3-((3-(4-((1,3-dioxolan-2-yl)methyl)phenyl)-1,2,4-oxadiazol-5-yl)methoxy)phenyl)(phenyl)methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine / ethanol; water / 16 h / 80 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C

2.2: 0.5 h / 150 °C / microwave irradiation

With hydroxylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; water; acetonitrile;