(HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh

Base Information

• Chemical Name: (HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh
• CAS No.: 1093122-53-2
• Molecular Formula: C₃₇H₄₆GeN₂
• Molecular Weight: 591.376
• Mol file: 1093122-53-2.mol

Synonyms:(HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh

Chemical Property of (HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh

Chemical Property:

Purity/Quality:

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Technology Process of (HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh

There total 1 articles about (HC[C(Me)N-2,6-iPr₂C₆H₃]₂)GeCCPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) + germanium(II) chloride-dioxane complex + lithium phenylacetylide (4440-01-1) → (HC[C(Me)N-2,6-iPr2C6H3]2)GeCCPh (1093122-53-2)

Guidance literature:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine; With n-butyllithium; In toluene; at -30 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

germanium(II) chloride-dioxane complex; In toluene; at -30 - 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

lithium phenylacetylide; In toluene; at -30 - 20 ℃; for 20h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om300724t

Reference yield: 91.0%

dodecacarbonyl-triangulo-triruthenium (15243-33-1) + (HC[C(Me)N-2,6-iPr2C6H3]2)GeCCPh (1093122-53-2) → C77H92Ge2N4O3Ru

Guidance literature:

In toluene; at 90 ℃; for 2h; Schlenk technique; Glovebox; Inert atmosphere;

DOI:10.1002/ejic.201700607

Reference yield: 74.0%

pentafluorophenyl copper tetramer + (HC[C(Me)N-2,6-iPr2C6H3]2)GeCCPh (1093122-53-2) + toluene (108-88-3,15644-74-3,16713-13-6) → (HC[C(Me)N-2,6-iPr2C6H3]2)Ge(CCPh)CuC6F5*toluene

Guidance literature:

In toluene; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om300724t

upstream raw materials:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

lithium phenylacetylide