2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

Base Information

Chemical Name:2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine
CAS No.:1053738-03-6
Molecular Formula:C₃₀H₄₉N₂O₁₀PSi₂
Molecular Weight:684.871
Hs Code.:

Synonyms:2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

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Chemical Property of 2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

Chemical Property:

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Technology Process of 2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

There total 4 articles about 2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1053749-13-5
Phosphoriodidic acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-(tert-butyl-dimethyl-silanyloxymethyl)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester ethyl ester

: 1053738-03-6
2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

Guidance literature:: With pyridine; In dichloromethane; at -30 ℃; for 0.25h; Yield given;
DOI:10.1021/jo00126a051

Reference yield:

: 169476-04-4
Phosphorous acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-(tert-butyl-dimethyl-silanyloxymethyl)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester diethyl ester

: 1053738-03-6
2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

Guidance literature:: Multi-step reaction with 2 steps

1: I₂, Cl^(1-), pyridine / CH₂Cl₂ / 0.17 h / 0 °C

2: pyridine / 16 h

With pyridine; chloride; iodine; In dichloromethane;
DOI:10.1021/jo00126a051

Reference yield:

: 54925-66-5
2',5'-bis-O-(tert-butyldimethylsilyl)uridine

: 1053738-03-6
2',5'-Di(tert-butyldimethylsilyl)-3'-(ethyl 4-formylphenyl phosphate)uridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0.17 h / 0 °C

2: I₂, Cl^(1-), pyridine / CH₂Cl₂ / 0.17 h / 0 °C

3: pyridine / 16 h

With pyridine; chloride; iodine; In dichloromethane;
DOI:10.1021/jo00126a051