adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene

Base Information

• Chemical Name: adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene
• CAS No.: 918621-09-7
• Molecular Formula: C₁₈F₁₂Hg₃*C₂₁H₃₀Si₃
• Molecular Weight: 1412.67
• Mol file: 918621-09-7.mol

Synonyms:adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene

Chemical Property of adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene

There total 1 articles about adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,3,5-tris-(1-trimethylsilylethynyl)benzene (18772-58-2) + perfluoro-o-phenylenemercury trimer (18734-63-9) → adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene (918621-09-7)

Guidance literature:

In tetrahydrofuran; mixt. dissolved in THF; solvent slowly evapd., washed twice with CH2Cl2; elem. anal.;

DOI:10.1002/anie.200602440

Reference yield:

adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene (918621-09-7) + n-butane (106-97-8,9003-29-6,9021-92-5) → adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene.cntd.0.71 n-butane

Guidance literature:

In neat (no solvent); exposure of adduct to atmosphere of alkane; detd. gravimetrically;

DOI:10.1002/anie.200602440

Reference yield:

adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene (918621-09-7) + pentane (109-66-0,8031-35-4,9078-70-0) → adduct of perfluoro-ortho-phenylene mercury and 1,3,5-tris(trimethylsilylethynyl)benzene.cntnd.0.45 n-pentane

Guidance literature:

In neat (no solvent); exposure to an atmosphere of pentane; detd. gravimetrically;

DOI:10.1002/anie.200602440

upstream raw materials:

1,3,5-tris-(1-trimethylsilylethynyl)benzene

perfluoro-o-phenylenemercury trimer