methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

Base Information

Chemical Name:methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate
CAS No.:853182-31-7
Molecular Formula:C₂₀H₂₅FO₄
Molecular Weight:348.415
Hs Code.:

Synonyms:methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

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Chemical Property of methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

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Technology Process of methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

There total 1 articles about methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122549-26-2
methyl 2-(4-fluorophenyl)methylidene-3-oxo-4-methylpentanoate

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 853182-31-7
methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

Guidance literature:: cyclohexanone; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 0 ℃; for 0.25h;

methyl 2-(4-fluorophenyl)methylidene-3-oxo-4-methylpentanoate; In tetrahydrofuran; at -78 ℃; for 3h;

Reference yield:

: 853182-31-7
methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate

: 853182-29-3
methyl 4-(4-fluorophenyl)-2-(1-methylethyl)-5,6,7,8-tetrahydroquinoline-3-carboxylate

Guidance literature:: methyl 4-fluoro-α-(1-oxo-2-methylpropyl)-β-(2-oxocyclohexyl)benzenepropanoate; With ammonium acetate; toluene-4-sulfonic acid; In ethanol; for 14h; Heating / reflux;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h;