3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

Base Information

Chemical Name:3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal
CAS No.:122805-03-2
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

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Chemical Property of 3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

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Technology Process of 3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

There total 3 articles about 3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 122776-11-8
5-(3-phenyl-2-propenyloxy)-6-methyl-3,4-bis(hydroxymethyl)pyridine hydrochloride

: 122805-03-2
3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

Guidance literature:: With manganese(IV) oxide; In acetone; at 40 ℃; for 1h;

Reference yield:

: 58-56-0
pyridoxal hydrochloride

: 122805-03-2
3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide, KI, 2.) HCl(gas) / 1.) acetone, reflux, 10 h, 2.) EtOH

2: 92 percent / MnO₂ / acetone / 1 h / 40 °C

With hydrogenchloride; manganese(IV) oxide; sodium ethanolate; potassium iodide; In acetone;

Reference yield:

: 4392-24-9
Cinnamyl bromide

: 122805-03-2
3-(3-phenyl-2-propenyloxy)-5-hydroxymethyl-2-methyl-4-pyridinecarboxaldehyde hemiacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide, KI, 2.) HCl(gas) / 1.) acetone, reflux, 10 h, 2.) EtOH

2: 92 percent / MnO₂ / acetone / 1 h / 40 °C

With hydrogenchloride; manganese(IV) oxide; sodium ethanolate; potassium iodide; In acetone;