phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate

Base Information

• Chemical Name: phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate
• CAS No.: 1225542-40-4
• Molecular Formula: C₁₄H₁₆N₂O₆
• Molecular Weight: 308.291

Synonyms:phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate

Chemical Property of phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate

Chemical Property:

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Technology Process of phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate

There total 1 articles about phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3-aminoisoxazol-5-yl)-2-hydroxymethylpropane-1,3-diol (1225542-39-1) + phenyl chloroformate (1885-14-9) → phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate (1225542-40-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃;

Reference yield:

2-(4-aminophenyl)-7-(2-morpholin-4-ylethoxy)imidazo[2,1-b][1,3]benzothiazole (950769-61-6) + phenyl 5-(1,3-dihydroxy-2-hydroxymethylpropan-2-yl)isoxazol-3-ylcarbamate (1225542-40-4) → 1-(5-(2-hydroxy-1,1-bis(hydroxymethyl)ethyl)isoxazol-3-yl)-3-(4-(7-(2-morpholin-4-ylethoxy)benzo[d]imidazo[2,1-b]thiazol-2-yl)phenyl)urea (1225542-14-2)

Guidance literature:

With dmap; In tetrahydrofuran; at 20 - 50 ℃;

upstream raw materials:

2-(3-aminoisoxazol-5-yl)-2-hydroxymethylpropane-1,3-diol

phenyl chloroformate

Downstream raw materials:

1-(5-(2-hydroxy-1,1-bis(hydroxymethyl)ethyl)isoxazol-3-yl)-3-(4-(7-(2-morpholin-4-ylethoxy)benzo[d]imidazo[2,1-b]thiazol-2-yl)phenyl)urea

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