2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester

Base Information

• Chemical Name: 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester
• CAS No.: 1065330-27-9
• Molecular Formula: C₁₈H₂₄O₄
• Molecular Weight: 304.386

Synonyms:2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester

Chemical Property of 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester

Chemical Property:

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Technology Process of 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester

There total 2 articles about 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

chloromethyl methyl ether (107-30-2) + (+/-)-1-phenyl-2-butylcycloprop-2-ene-1-carboxylic acid (678195-44-3) → 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester (1065330-27-9)

Guidance literature:

(+/-)-1-phenyl-2-butylcycloprop-2-ene-1-carboxylic acid; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 - 5 ℃; for 0.216667h;

chloromethyl methyl ether; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.5h;

With hydrogenchloride; water; In tetrahydrofuran; diethyl ether; pH=1 - 2;

DOI:10.1021/jo801683n

Reference yield:

chloromethyl methyl ether (107-30-2) + diazomethyl-trimethyl-silane (18107-18-1) + (+/-)-1-phenyl-2-butylcycloprop-2-ene-1-carboxylic acid (678195-44-3) → 2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester (1065330-27-9) + C17H22O3

Guidance literature:

(+/-)-1-phenyl-2-butylcycloprop-2-ene-1-carboxylic acid; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.0833333h;

chloromethyl methyl ether; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 1h;

diazomethyl-trimethyl-silane; In methanol; hexane; at 0 ℃; Cooling with ice;

DOI:10.1055/s-0033-1338876

Reference yield:

2-butyl-3-methoxymethyl-1-phenyl-cycloprop-2-ene-1-carboxylic acid methoxymethyl ester (1065330-27-9) + C17H22O3 → 2-butyl-1-(hydroxymethyl)-1-phenyl-3-(methoxymethyl)cycloprop-2-ene (1450906-55-4)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃; for 2.16667h;

DOI:10.1055/s-0033-1338876

upstream raw materials:

chloromethyl methyl ether

(+/-)-1-phenyl-2-butylcycloprop-2-ene-1-carboxylic acid

diazomethyl-trimethyl-silane

Downstream raw materials:

2-butyl-1-(hydroxymethyl)-1-phenyl-3-(methoxymethyl)cycloprop-2-ene

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