C₂₈H₃₄O₅

Base Information

Chemical Name:C₂₈H₃₄O₅
CAS No.:827325-42-8
Molecular Formula:C₂₈H₃₄O₅
Molecular Weight:450.575
Hs Code.:

C<sub>28</sub>H<sub>34</sub>O<sub>5</sub>

Synonyms:C₂₈H₃₄O₅

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Chemical Property of C₂₈H₃₄O₅

Chemical Property:

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Technology Process of C₂₈H₃₄O₅

There total 9 articles about C₂₈H₃₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 827325-41-7
C₂₈H₃₄O₄

: 827325-42-8
C₂₈H₃₄O₅

Guidance literature:: With potassium tert-butylate; oxygen; phosphorous acid trimethyl ester; In tetrahydrofuran; tert-butyl alcohol; at -40 ℃; for 0.75h;
DOI:10.1021/ja044123l

Reference yield:

: 454482-62-3
1-(((2-(chloromethyl)allyl)oxy)methyl)-4-methoxybenzene

: 827325-42-8
C₂₈H₃₄O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: 98 percent / KH / tetrahydrofuran / Heating

2.1: 76 percent / Hoveyda-Grubbs catalyst / toluene / 30 h / Heating

3.1: aq. HCl / tetrahydrofuran / 3 h / Heating

4.1: 1.9 g / NaBH₄ / ethanol; tetrahydrofuran / 0.25 h / 0 °C

5.1: PPh₃; imidazole; I₂ / tetrahydrofuran / 3 h / 0 °C

5.2: 94 percent / t-BuOK / tetrahydrofuran; dimethylsulfoxide / 20 °C

6.1: 49 percent / SeO₂; aq. AcOH; t-BuOOH / CH₂Cl₂; decane / 2 h / 20 °C

7.1: 74 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / -40 - 10 °C

8.1: 74 percent / aq. RhCl₃ / aq. ethanol / 0.58 h / 115 °C

9.1: 94 percent / P(OMe)3; O₂; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C

With 1H-imidazole; hydrogenchloride; tert.-butylhydroperoxide; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; sodium tetrahydroborate; rhodium(III) chloride; selenium(IV) oxide; potassium tert-butylate; iodine; oxygen; potassium hydride; Dess-Martin periodane; acetic acid; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; decane; ethanol; dichloromethane; toluene; tert-butyl alcohol; 2.1: Grubbs reaction;
DOI:10.1021/ja044123l

Reference yield:

: C₂₈H₃₆O₄

: 827325-42-8
C₂₈H₃₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1.9 g / NaBH₄ / ethanol; tetrahydrofuran / 0.25 h / 0 °C

2.1: PPh₃; imidazole; I₂ / tetrahydrofuran / 3 h / 0 °C

2.2: 94 percent / t-BuOK / tetrahydrofuran; dimethylsulfoxide / 20 °C

3.1: 49 percent / SeO₂; aq. AcOH; t-BuOOH / CH₂Cl₂; decane / 2 h / 20 °C

4.1: 74 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / -40 - 10 °C

5.1: 74 percent / aq. RhCl₃ / aq. ethanol / 0.58 h / 115 °C

6.1: 94 percent / P(OMe)3; O₂; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium tetrahydroborate; rhodium(III) chloride; selenium(IV) oxide; potassium tert-butylate; iodine; oxygen; Dess-Martin periodane; acetic acid; triphenylphosphine; phosphorous acid trimethyl ester; In tetrahydrofuran; decane; ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ja044123l