N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

Base Information

Chemical Name:N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide
CAS No.:942509-21-9
Molecular Formula:C₂₂H₂₆BrNO₃S
Molecular Weight:464.423
Hs Code.:

Synonyms:N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

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Chemical Property of N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

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Technology Process of N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

There total 5 articles about N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 942509-20-8
N-[(Z)-3-bromo-3-methoxycarbonylprop-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

: 942509-21-9
N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo0700528

Reference yield:

: 942509-19-5
N-(2-hydroxyethyl)-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

: 942509-21-9
N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N; SO₃*Py / dimethylsulfoxide / 1 h / 20 °C

2: 1.47 g / CHCl₃ / 15 h / 20 °C

3: 85 percent / DIBAL-H / CH₂Cl₂; hexane / 1 h / 0 °C

With pyridine-SO₃ complex; diisobutylaluminium hydride; triethylamine; In hexane; dichloromethane; chloroform; dimethyl sulfoxide; 2: Wittig olefination;
DOI:10.1021/jo0700528

Reference yield:

: 1026910-12-2
C₂₀H₂₃SO₃N

: 942509-21-9
N-[(Z)-3-bromo-4-hydroxybut-2-enyl]-2,4,6-trimethyl-N-[(E)-3-phenylprop-2-enyl]phenylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.47 g / CHCl₃ / 15 h / 20 °C

2: 85 percent / DIBAL-H / CH₂Cl₂; hexane / 1 h / 0 °C

With diisobutylaluminium hydride; In hexane; dichloromethane; chloroform; 1: Wittig olefination;
DOI:10.1021/jo0700528