(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

Base Information

Chemical Name:(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol
CAS No.:474970-80-4
Molecular Formula:C₃₂H₅₀O₅SeSi
Molecular Weight:621.792
Hs Code.:

Synonyms:(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

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Chemical Property of (E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

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Technology Process of (E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

There total 7 articles about (E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1666-13-3
diphenyl diselenide

: 474970-79-1
{3-[(E)-5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-2-enyl]-5-methoxy-4-methoxymethoxy-benzyloxy}-triethyl-silane

: 474970-80-4
(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

Guidance literature:: With sodium tetrahydroborate;
DOI:10.1021/ol0266368

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 474970-80-4
(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / n-BuLi

2: 53 percent / mCPBA / cooling

3: 83 percent / NaBH₄

With sodium tetrahydroborate; n-butyllithium; 3-chloro-benzenecarboperoxoic acid;
DOI:10.1021/ol0266368

Reference yield:

: 994-30-9
triethylsilyl chloride

: 474970-80-4
(E)-8-(3-Methoxy-2-methoxymethoxy-5-triethylsilanyloxymethyl-phenyl)-2,6-dimethyl-3-phenylselanyl-oct-6-en-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / imidazole

2: 74 percent / n-BuLi

3: 53 percent / mCPBA / cooling

4: 83 percent / NaBH₄

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; 3-chloro-benzenecarboperoxoic acid;
DOI:10.1021/ol0266368