threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

Base Information

Chemical Name:threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol
CAS No.:1257993-01-3
Molecular Formula:C₂₄H₂₆O₇S
Molecular Weight:458.532
Hs Code.:

Synonyms:threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

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Chemical Property of threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

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Technology Process of threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

There total 6 articles about threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98-59-9
p-toluenesulfonyl chloride

: 300678-35-7
(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-2,3-dihydroxypropanol

: 1257993-01-3
threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1007/s00706-010-0420-3

Reference yield:

: 38153-27-4
(2E)-3-(4-O-benzyloxy-3-methoxyphenyl)prop-2-en-1-ol

: 1257993-01-3
threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: AD-mix-β; methanesulfonamide; water / tert-butyl alcohol / 0 °C

2: pyridine / dichloromethane / 20 °C

With pyridine; methanesulfonamide; AD-mix-β; water; In dichloromethane; tert-butyl alcohol;
DOI:10.1007/s00706-010-0420-3

Reference yield:

: 38157-08-3
(E)-3-(4-benzyloxy-3-methoxyphenyl)acrylic acid ethyl ester

: 1257993-01-3
threo-(1R,2R)-1-(4-benzyloxy-3-methoxyphenyl)-3-O-tosyl-1,2,3-propanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran

2: AD-mix-β; methanesulfonamide; water / tert-butyl alcohol / 0 °C

3: pyridine / dichloromethane / 20 °C

With pyridine; aluminum (III) chloride; lithium aluminium tetrahydride; methanesulfonamide; AD-mix-β; water; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;
DOI:10.1007/s00706-010-0420-3