(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

Base Information

Chemical Name:(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine
CAS No.:148065-96-7
Molecular Formula:C₁₈H₁₄N₈O
Molecular Weight:358.362
Hs Code.:

Synonyms:(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

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Chemical Property of (3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

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Technology Process of (3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

There total 3 articles about (3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 148065-95-6
10-Carbethoxymethyl-10H-3-phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indole

: 148065-96-7
(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; for 0.5h; Heating;
DOI:10.1002/ardp.19933260307

Reference yield:

: 113306-13-1
3-Phenyl-10H-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indole

: 148065-96-7
(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃ / dimethylformamide; acetone / 6 h / Heating

2: 90 percent / 99percent N₂H₄*H₂O / dimethylformamide / 0.5 h / Heating

With potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/ardp.19933260307

Reference yield:

: 113306-10-8
3-(Benzylidenehydrazono)-5H-<1,2,4>triazino<5,6-b>indole

: 148065-96-7
(3-Phenyl-1,2,4-triazolo<4',3':2,3><1,2,4>triazino<5,6-b>indol-10-yl)acetylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: FeCl₃ / ethanol / 1) 10 h, reflux, 2) r.t., overnight

2: 90 percent / K₂CO₃ / dimethylformamide; acetone / 6 h / Heating

3: 90 percent / 99percent N₂H₄*H₂O / dimethylformamide / 0.5 h / Heating

With iron(III) chloride; potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1002/ardp.19933260307