Cp*ZrI(μ-OCH2Ph2P)2PtMe2

Base Information

• Chemical Name: Cp*ZrI(μ-OCH2Ph2P)2PtMe2
• CAS No.: 113646-86-9
• Molecular Formula: C₃₈H₄₅IO₂P₂PtZr
• Molecular Weight: 1008.93

Synonyms:Cp*ZrI(μ-OCH2Ph2P)2PtMe2

Chemical Property of Cp*ZrI(μ-OCH2Ph2P)2PtMe2

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Technology Process of Cp*ZrI(μ-OCH2Ph2P)2PtMe2

There total 1 articles about Cp*ZrI(μ-OCH2Ph2P)2PtMe2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

cis-Cp*ZrMe(μOCH2Ph2P)2 (113646-88-1) → Cp*ZrI(μ-OCH2Ph2P)2PtMe2 (113646-86-9)

Guidance literature:

With methyl iodide; In benzene; condensing methyl iodide to cis-Cp*ZrMe(μOCH2Ph2P)2PtMe2 in benzene at -196°C, heating (92°C, 10 h); reducing vol., adding hexane, pptn., triturating with hexane, filtration, washing (hexane), drying in vacuo; 1H NMR spectrum, 31P (1H) NMR spectrum;

DOI:10.1021/ja00221a024

upstream raw materials:

cis-Cp*ZrMe(μOCH2Ph2P)2

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