Technology Process of C19H23N3O4
There total 6 articles about C19H23N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / methanol / 15 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / methanol / 20 °C
3: acetic acid / N,N-dimethyl-formamide / 0.08 h / 150 °C / Microwave irradiation
4: triethylamine / dichloromethane / 24 h / 0 - 20 °C
5: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 1 h / 20 °C
With
palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium tert-butylate / 12 h / -10 - 20 °C / Inert atmosphere; Large scale
2: potassium carbonate / methanol / 15 h / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 20 °C
4: acetic acid / N,N-dimethyl-formamide / 0.08 h / 150 °C / Microwave irradiation
5: triethylamine / dichloromethane / 24 h / 0 - 20 °C
6: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 1 h / 20 °C
With
palladium 10% on activated carbon; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;