Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃

Base Information

• Chemical Name: Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃
• CAS No.: 470663-73-1
• Molecular Formula: CF₃O₃S*C₄₄H₄₂IrN₂P₂
• Molecular Weight: 1002.07

Synonyms:Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃

Chemical Property of Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃

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Technology Process of Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃

There total 1 articles about Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CH₃CN)2(P(C₆H₅)3)2CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

[IrH2(P(C6H5)3)2(CH3CN)2](1+)*CF3SO3(1-)=[IrH2(P(C6H5)3)2(CH3CN)2][CF3SO3] (470663-71-9) + acetylene (74-86-2,25067-58-7) → Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2CF3SO3 (470663-73-1)

Guidance literature:

In dichloromethane; Ir-complex in CH2Cl2 was stirred under CHCH (1 atm) at 0°C for 5 h; filtered, washed with n-pentane, dried under vac.; elem. anal.;

DOI:10.1021/om020410r

Reference yield: 98.0%

Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CH3CN)2(P(C6H5)3)2CF3SO3 (470663-73-1) + carbon monoxide (201230-82-2) → Ir(CHCH2)2(CO)2(P(C6H5)3)2(1+)*CF3SO3(1-)=Ir(CHCH2)2(CO)2(P(C6H5)3)2CF3SO3 (470663-75-3)

Guidance literature:

In dichloromethane; byproducts: CH3CN; Ir-complex in CH2Cl2 was stirred under CO (1 atm) at 25°C for 3 h, n-pentane was added; filtered, washed with n-pentane, dried under vac.; elem. anal.;

DOI:10.1021/om020410r

Reference yield: 98.0%

[Ir(-CH=CH2)2(NCCH3)2(PPh3)2]OTf (470663-73-1) + triethylamine (121-44-8) + acetylene (74-86-2,25067-58-7) → [Ir(-CH=CHNEt3)(η4-CH2=CHCH=CH2)(PPh3)2]OTf (540535-67-9)

Guidance literature:

In chloroform; soln. Ir complex in CHCl3 and NEt2 was stirred under HCCH (1 atm) at 25°Cfor 1 h; react. mixt. was extd. with water, pentane was added, ppt. was filtered,washed with cold pentane and dried under vac.; elem. anal.;

DOI:10.1021/om030090r

upstream raw materials:

[IrH₂(P(C₆H₅)3)2(CH₃CN)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[IrH₂(P(C₆H₅)3)2(CH₃CN)2][CF₃SO₃]

acetylene

Downstream raw materials:

Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(CHCH₂)2(CO)2(P(C₆H₅)3)2CF₃SO₃

[Ir(-CH=CHNEt3)(η4-CH2=CHCH=CH2)(PPh3)2]OTf

Ir(CH=CH2)2(η2-O2CCH3)(PPh3)2

[Ir(η4-CH2=CHCH=CH2)(CH3CN)(PPh3)2]OTf

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