Technology Process of C23H28N4O2
There total 4 articles about C23H28N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H25N3O2; phenyl isothiocyanate;
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
With
dicyclohexyl-carbodiimide;
In
tetrahydrofuran;
at 60 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 0.5 h / -78 °C
1.2: 20 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 100 °C / Inert atmosphere
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
4.1: triethylamine / tetrahydrofuran / 20 °C
4.2: 2 h / 60 °C
With
hydrogen; sodium carbonate; triethylamine; lithium diisopropyl amide;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; n-heptane; ethylbenzene; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 100 °C / Inert atmosphere
2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
3.1: triethylamine / tetrahydrofuran / 20 °C
3.2: 2 h / 60 °C
With
hydrogen; sodium carbonate; triethylamine;
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;
