3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

Base Information

Chemical Name:3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide
CAS No.:304863-14-7
Molecular Formula:C₅₄H₇₉N₅O₈S₄
Molecular Weight:1054.51
Hs Code.:

Synonyms:3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

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Chemical Property of 3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

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Technology Process of 3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

There total 5 articles about 3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5332-06-9
4-bromobutanenitrile

: 304863-12-5
1,6,11,16-tetrakis(mesitylenesulfonyl)-6,11,16-tetraaza-1-heptadecylamine

: 304863-14-7
3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

Guidance literature:: 1,6,11,16-tetrakis(mesitylenesulfonyl)-6,11,16-tetraaza-1-heptadecylamine; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

4-bromobutanenitrile; In N,N-dimethyl-formamide; at 22 ℃; for 18h;
DOI:10.1021/jm030175u

Reference yield:

: 161452-20-6
1,6,11-tris(mesitylenesulfonyl)-1,6,11-triazatridecane

: 304863-14-7
3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / dimethylformamide / 0.5 h

1.2: 97 percent / dimethylformamide / 18 h / 22 °C

2.1: 94 percent / H₂ / PtO₂ / CHCl₃; ethanol / 5 h / 2327.17 Torr

3.1: 79 percent / aq. NaOH / CHCl₃ / 18 h / 22 °C

4.1: NaH / dimethylformamide / 0.5 h

4.2: 98 percent / dimethylformamide / 18 h / 22 °C

With sodium hydroxide; hydrogen; sodium hydride; platinum(IV) oxide; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm030175u

Reference yield:

: 304863-09-0
3,8,13-tris(mesitylenesulfonyl)-3,8,13-triazahexadecylcyanide

: 304863-14-7
3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaheneicosanecyanide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / H₂ / PtO₂ / CHCl₃; ethanol / 5 h / 2327.17 Torr

2.1: 79 percent / aq. NaOH / CHCl₃ / 18 h / 22 °C

3.1: NaH / dimethylformamide / 0.5 h

3.2: 98 percent / dimethylformamide / 18 h / 22 °C

With sodium hydroxide; hydrogen; sodium hydride; platinum(IV) oxide; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm030175u