C₂₄H₂₆OS

Base Information

• Chemical Name: C₂₄H₂₆OS
• CAS No.: 1290137-51-7
• Molecular Formula: C₂₄H₂₆OS
• Molecular Weight: 362.536
• Mol file: 1290137-51-7.mol

Synonyms:C₂₄H₂₆OS

Chemical Property of C₂₄H₂₆OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₆OS

There total 1 articles about C₂₄H₂₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

5-bromopentan-1-ol (34626-51-2) + triphenylmethanethiol (3695-77-0) → C24H26OS (1290137-51-7)

Guidance literature:

With sodium hydroxide; In ethanol; water; toluene; at 70 ℃; for 6h;

DOI:10.1039/c0cc04975a

Reference yield: 99.0%

C24H26OS (1290137-51-7) + methanesulfonyl chloride (124-63-0) → C25H28O3S2 (1290137-53-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/c0cc04975a

Reference yield:

C24H26OS (1290137-51-7) → C32H42O5S (1290137-55-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / dichloromethane; water / 90 - 100 °C

2.2: 24 h / 90 - 100 °C

With triethylamine; sodium hydroxide; In dichloromethane; water;

DOI:10.1039/c0cc04975a

upstream raw materials:

5-bromopentan-1-ol

triphenylmethanethiol

Downstream raw materials:

C₃₂H₄₂O₅S

C₂₅H₂₈O₃S₂