2,6-diisopropylphenylimino-thexylborane

Base Information

Chemical Name:2,6-diisopropylphenylimino-thexylborane
CAS No.:109874-47-7
Molecular Formula:C₁₈H₃₀BN
Molecular Weight:271.254
Hs Code.:

Synonyms:2,6-diisopropylphenylimino-thexylborane

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Chemical Property of 2,6-diisopropylphenylimino-thexylborane

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Technology Process of 2,6-diisopropylphenylimino-thexylborane

There total 1 articles about 2,6-diisopropylphenylimino-thexylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: bromo-(2,6-diisopropylphenylamino)thexylborane

: 109874-47-7
2,6-diisopropylphenylimino-thexylborane

Guidance literature:: With n-butyllithium; In hexane; byproducts: lithium bromide; N2 atm.; addn. of soln. of TMP to n-BuLi in hexane, reflux for 3h; soln. added to thexylborane compd.; stirring overnight, reflux for 4h; distn. of solvent in low vac.; distn. in high vac.; distn.; elem. anal.;
DOI:10.1016/0022-328X(86)80212-1

Reference yield: 85.0%

: 109874-47-7
2,6-diisopropylphenylimino-thexylborane

: 109874-48-8
hydroxy-2,6-diisopropylphenylamino-thexylborane

Guidance literature:: With water; In dichloromethane; N2 atm., addn. of H2O to soln. of borane compd. in CH2Cl2, stirring at 20°C for 3d; removal of solvent in vac.; sublimation in vac.; elem. anal.;
DOI:10.1016/0022-328X(86)80212-1

Reference yield: 76.0%

: 109874-47-7
2,6-diisopropylphenylimino-thexylborane

: 75-64-9
tert-butylamine

: 109874-49-9
t-butylamino-2,6-diisopropylphenylamino-thexylborane

Guidance literature:: In dichloromethane; under N2 atm., addn. of Me3CNH2 to soln. of borane compd. in CH2Cl2 at 20°C; stirring overnight, refluxing for 8h; removal of solvent in vac.; distn. in vac.;
DOI:10.1016/0022-328X(86)80212-1