Technology Process of C23H27(2)HINO2S
There total 4 articles about C23H27(2)HINO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate;
In
toluene;
at 120 ℃;
for 16h;
stereospecific reaction;
Inert atmosphere;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
3: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; di-isopropyl azodicarboxylate; palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; toluene;
1: Mitsunobu reaction / 2: Mitsunobu reaction;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere
1.2: 3 h / -78 - 20 °C / Inert atmosphere
1.3: Saturated solution
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
4.1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate / toluene / 16 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; di-isopropyl azodicarboxylate; palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; toluene;
2.1: Mitsunobu reaction / 3.1: Mitsunobu reaction;
DOI:10.1021/ja201204g
