2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole

Base Information

• Chemical Name: 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole
• CAS No.: 189942-78-7
• Molecular Formula: C₂₀H₂₁Cl₂F₃O₂
• Molecular Weight: 421.287

Synonyms:2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole

Chemical Property of 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole

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Technology Process of 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole

There total 1 articles about 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.1%

diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate (220417-58-3) + 5-chloroadamantan-2-one (20098-17-3) → 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.13,7]dec-2-ylidenemethyl)} anisole (189942-78-7)

Guidance literature:

diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.583333h;

5-chloroadamantan-2-one; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.55h; Heating / reflux;

With water; sodium hydrogencarbonate; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 100.0%

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.13,7]dec-2-ylidenemethyl)} anisole (189942-78-7) → 2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.13,7]dec-2-ylidenemethyl)}phenol (189942-79-8)

Guidance literature:

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole; With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; at 0 - 108 ℃; for 3.25h;

With water; sodium hydrogencarbonate; In N,N-dimethyl-formamide;

upstream raw materials:

diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

5-chloroadamantan-2-one

Downstream raw materials:

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)}phenol

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