N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

Base Information

Chemical Name:N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide
CAS No.:1358577-95-3
Molecular Formula:C₂₂H₁₃Cl₄N₅O₆S₂
Molecular Weight:649.319
Hs Code.:

Synonyms:N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

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Technology Process of N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

There total 4 articles about N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 16271-33-3
2,4-Dichlorobenzenesulfonyl chloride

: 36303-46-5
6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diamine

: 1358577-95-3
N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2011.12.033

Reference yield:

: 2089-36-3,20747-41-5,20747-42-6
(E)-3,4-methylenedioxybenzaldehyde oxime

: 1358577-95-3
N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / Reflux

2: potassium hydroxide / water / Reflux

3: triethylamine / dichloromethane / 0 - 20 °C

With acetic anhydride; triethylamine; potassium hydroxide; In dichloromethane; water;
DOI:10.1016/j.ejmech.2011.12.033

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1358577-95-3
N,N'-(6-(1,3-benzodioxol-5-yl)-1,3,5-triazine-2,4-diyl)-bis-2,4-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / water

2: acetic anhydride / Reflux

3: potassium hydroxide / water / Reflux

4: triethylamine / dichloromethane / 0 - 20 °C

With hydroxylamine hydrochloride; acetic anhydride; sodium hydrogencarbonate; triethylamine; potassium hydroxide; In dichloromethane; water;
DOI:10.1016/j.ejmech.2011.12.033