2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

Base Information

Chemical Name:2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate
CAS No.:160290-96-0
Molecular Formula:C₁₁H₈F₃N₃O₄
Molecular Weight:303.197
Hs Code.:

Synonyms:2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

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Chemical Property of 2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

Chemical Property:

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Technology Process of 2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

There total 3 articles about 2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 160290-95-9
1-bromo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>acetone

: 160290-96-0
2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

Guidance literature:: With silver nitrate; In acetonitrile; for 38h; Ambient temperature;
DOI:10.1039/c39940002405

Reference yield:

: 148058-40-6
2-(4-(3-(trifluoromethyl)-3H-diazirin-3-yl)phenyl)acetic acid

: 160290-96-0
2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₁ / benzene / 14 h / Ambient temperature

2: diethyl ether / 0.83 h / 0 °C

3: 86 percent / HBr gas / diethyl ether / 0.5 h / 0 °C

4: 88 percent / AgNO₃ / acetonitrile / 18 h / Ambient temperature

With thionyl chloride; hydrogen bromide; silver nitrate; In diethyl ether; acetonitrile; benzene;

Reference yield:

: 160290-94-8
1-azo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>acetone

: 160290-96-0
2-oxo-3-<4-(3-fluoromethyldiazirin-3-yl)phenyl>propyl nitrate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / HBr gas / diethyl ether / 0.5 h / 0 °C

2: 88 percent / AgNO₃ / acetonitrile / 18 h / Ambient temperature

With hydrogen bromide; silver nitrate; In diethyl ether; acetonitrile;