3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Base Information

Chemical Name:3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate
CAS No.:647830-31-7
Molecular Formula:C₂₆H₂₄Cl₃NO₁₀
Molecular Weight:616.836
Hs Code.:

Synonyms:3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Suppliers and Price of 3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

There total 2 articles about 3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 545-06-2
trichloroacetonitrile

: 3,6-di-O-acetyl-2,4-di-O-benzoyl-D-mannopyranose

: 647830-31-7
3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2003.09.219

Reference yield:

: 647830-29-3
C₂₄H₂₅NO₉

: 647830-31-7
3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / HCl; NaNO₂ / acetone; H₂O / 0.67 h / 0 - 20 °C

2: 90 percent / DBU / 1 h / 0 - 20 °C

With hydrogenchloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium nitrite; In water; acetone;
DOI:10.1016/j.tetlet.2003.09.219