methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

Base Information

Chemical Name:methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate
CAS No.:288852-11-9
Molecular Formula:C₃₁H₃₃NO₈
Molecular Weight:547.605
Hs Code.:

Synonyms:methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

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Chemical Property of methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

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Technology Process of methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

There total 8 articles about methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 93-97-0
benzoic acid anhydride

: 288852-09-5
methyl 2-((2S,3S)-2-hydroxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

: 288852-11-9
methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 24h;
DOI:10.1021/ol990320r

Reference yield: 64.0%

: 65-85-0,8013-63-6
benzoic acid

: 288852-10-8
methyl 2-((2R,3S)-2-hydroxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

: 288852-11-9
methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

Guidance literature:: With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol990320r

Reference yield:

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 288852-11-9
methyl 2-((2S,3S)-2-benzoyloxy-4-(4-methoxyphenyl)methoxy-3-(N-phenylmethoxycarbonyl)amino)butylpropenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / indium / tetrahydrofuran; H₂O / 4.5 h

2: 64 percent / di-tert-butyl azodicarboxylate; Ph₃P / tetrahydrofuran / 20 °C

With indium; di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; water; 1: Condensation / 2: Mitsunobu reaction;
DOI:10.1021/ol990320r