3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid

Base Information

• Chemical Name: 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid
• CAS No.: 114072-73-0
• Molecular Formula: C₁₉H₂₀O₆
• Molecular Weight: 344.364

Synonyms:3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid

Chemical Property of 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid

Chemical Property:

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Technology Process of 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid

There total 15 articles about 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

3-[4-(2-Hydroxy-3,4-dimethoxy-6-methyl-benzyl)-phenyl]-propionic acid (114072-84-3) → 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid (114072-73-0)

Guidance literature:

With salcomine; oxygen; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

DOI:10.1248/cpb.44.139

Reference yield: 50.0%

→ N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]piperidine (245086-31-1) + 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid (114072-73-0)

Guidance literature:

Reference yield: 29.0%

→ N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]ethanolamine (245086-34-4) + 3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionic acid (114072-73-0)

Guidance literature:

upstream raw materials:

3-[4-(2-Hydroxy-3,4-dimethoxy-6-methyl-benzyl)-phenyl]-propionic acid

p-bromobenzaldehyde 1,3-dioxolane

2-hydroxy-3,4-dimethoxy-6-methylbenzaldehyde

2-{4-[hydroxy-(3,4-dimethoxy-2-hydroxy-6-methyl)phenyl]methylphenyl}-1,3-dioxolane

Downstream raw materials:

N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]piperidine

N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]thiomorpholine

N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]benzylamine

N-[3-[4-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-ylmethyl)phenyl]propionyl]dimethylamine

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