phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside
CAS No.:1385808-41-2
Molecular Formula:C₆₆H₆₈N₆O₈S
Molecular Weight:1105.37
Hs Code.:

phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

Synonyms:phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

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Chemical Property of phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

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Technology Process of phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

There total 4 articles about phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1201639-31-7
3',6'-bis(diethylamino)-2-(prop-2-yn-1-yl)spiro[isoindoline-1,9'-xanthen]-3-one

: 1385808-26-3
phenyl 6-O-(2-azido)acetyl-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

: 1385808-41-2
phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; at 20 ℃;
DOI:10.1055/s-0031-1290975

Reference yield:

: 819798-14-6
phenyl 2,3,4-tri-O-benzyl-6-O-chloroacetyl-1-thio-β-D-galactopyranoside

: 1385808-41-2
phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; potassium iodide / acetone / 24 h / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; potassium iodide; In dichloromethane; acetone; 2: Huisgen cycloaddition;
DOI:10.1055/s-0031-1290975

Reference yield:

: 38184-12-2,120403-26-1,87470-73-3
phenyl 2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

: 1385808-41-2
phenyl 2,3,4-tri-O-benzyl-6-O-[2-(4-{[3',6'-bis(diethylamino)-3-oxospiro(isoindoline-1,9'-xanthene)-2-yl]methyl}-1H-1,2,3-triazol-1-yl)]acetyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 14 h / 0 - 20 °C

2: sodium azide; potassium iodide / acetone / 24 h / 20 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; potassium iodide; In dichloromethane; acetone; 3: Huisgen cycloaddition;
DOI:10.1055/s-0031-1290975