((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

Base Information

Chemical Name:((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane
CAS No.:1443751-17-4
Molecular Formula:C₂₄H₂₈O₄Si
Molecular Weight:408.569
Hs Code.:

Synonyms:((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

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Technology Process of ((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

There total 2 articles about ((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 534-22-5
2-methylfuran

: 1443750-85-3
(4,5-dimethoxy-2-((trimethylsilyl)ethynyl)phenyl)(5-methylfuran-2-yl)methanol

: 1443751-17-4
((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

Guidance literature:: With perchloric acid; In 1,4-dioxane; water; at 0 - 20 ℃; for 0.166667h;
DOI:10.1002/chem.201202004

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1443751-17-4
((2-(bis(5-methylfuran-2-yl)methyl)-4,5-dimethoxyphenyl)ethynyl)trimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 16 h / 65 °C

2.1: n-butyllithium / diethyl ether; tetrahydrofuran / 3 h / 0 - 20 °C

2.2: 6 h / 0 - 20 °C

3.1: perchloric acid / 1,4-dioxane; water / 0.17 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; perchloric acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; 1.1: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201202004