11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

Base Information

Chemical Name:11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione
CAS No.:1432795-55-5
Molecular Formula:C₃₀H₃₈O₈S
Molecular Weight:558.693
Hs Code.:

Synonyms:11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

Chemical Property:

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Technology Process of 11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

There total 2 articles about 11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 11,21-dihydroxy-17-[1-oxo-3-(phenylthio)propoxy]-(11β)-pregn-4-ene-3,20-dione

: 1432795-55-5
11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2h; Cooling with ice;

Reference yield:

: 50-23-7
HYDROCORTISONE

: 342885-78-3
1,1-diethoxy-3-(phenylsulfenyl)propyl ethyl ether

: 1432795-55-5
11,21-dihydroxy-17-[1-oxo-3-(phenylsulfonyl)propoxy]-(11β)-pregn-4-ene-3,20-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / tetrahydrofuran / 3 h / 70 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / Cooling with ice

With pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;