2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

Base Information

Chemical Name:2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester
CAS No.:1025942-31-7
Molecular Formula:C₁₇H₂₀O₉
Molecular Weight:368.34
Hs Code.:

Synonyms:2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

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Chemical Property of 2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

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Technology Process of 2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

There total 4 articles about 2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 117379-88-1
4-acetoxy-3-bromomethyl-benzoic acid methyl ester

: 70681-41-3
(R)-dimethyl malate

: 1025942-31-7
2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

Guidance literature:: With silver(l) oxide; In diethyl ether; for 45.5h;
DOI:10.1039/b503802b

Reference yield:

: 863886-93-5
4-acetoxy-3-methyl-benzoic acid methyl ester

: 1025942-31-7
2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / N-bromosuccinimide; AIBN / benzene / 6 h / 85 °C

2: 37 percent / Ag₂O / diethyl ether / 45.5 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); silver(l) oxide; In diethyl ether; benzene;
DOI:10.1039/b503802b

Reference yield:

: 499-76-3
4-hydroxy-3-methylbenzoic acid

: 1025942-31-7
2-(2-acetoxy-5-methoxycarbonyl-(R)-benzyloxy)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / SOCl₂ / 16 h / Heating

2: 76 percent / pyridine / 6 h / 22 °C

3: 79 percent / N-bromosuccinimide; AIBN / benzene / 6 h / 85 °C

4: 37 percent / Ag₂O / diethyl ether / 45.5 h

With pyridine; N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); silver(l) oxide; In diethyl ether; benzene;
DOI:10.1039/b503802b