1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride

Base Information

• Chemical Name: 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride
• CAS No.: 1228185-08-7
• Molecular Formula: C₃₄H₄₁N₂O*Cl
• Molecular Weight: 529.165

Synonyms:1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride

Chemical Property of 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride

Chemical Property:

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SDS file from LookChem

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Technology Process of 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride

There total 2 articles about 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

benzoyl chloride (98-88-4) + 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene (244187-81-3) → 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride (1228185-08-7)

Guidance literature:

In hexane; at 20 ℃; Inert atmosphere; Glovebox; Schlenk technique;

DOI:10.1039/c5cc06322a

Reference yield:

1,3-bis(2,6-diisopropylphenyl)-2,4-dibenzoylimidazolium chloride (1228185-22-5) + 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene (244187-81-3) → 1,3-bis(2,6-diisopropylphenyl)-4-benzoylimidazol-2-ylidene (1228185-16-7) + 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride (1228185-08-7)

Guidance literature:

In diethyl ether; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja102639a

Reference yield: 73.0%

N,N-bis(2,6-diisopropylphenyl)-2,4-diphenylimidazol-5-ylidene-1-ium (1201311-20-7) + 1,3-bis(2,6-diisopropylphenyl)-2-benzoylimidazolium chloride (1228185-08-7) → C46H49N2O(1+)*Cl(1-) (1228185-25-8) + 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene (244187-81-3)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ja102639a

upstream raw materials:

1,3-bis(2,6-diisopropylphenyl)-2,4-dibenzoylimidazolium chloride

1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

benzoyl chloride

Downstream raw materials:

C₄₆H₄₉N₂O⁽¹⁺⁾*Cl^(1-)

1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

1,3-bis(2,6-diisopropylphenyl)-4-benzoylimidazol-2-ylidene

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