(1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one

Base Information

• Chemical Name: (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one
• CAS No.: 251950-67-1
• Molecular Formula: C₃₇H₅₂O₁₁
• Molecular Weight: 672.813

Synonyms:(1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one

Chemical Property of (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one

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Technology Process of (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one

There total 1 articles about (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.0^4,9]pentadecan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(2'R,4S,4'S,4'aS,6'R,7'S,10'S,11'S,12'aS)-4'-[(Benzyloxy)methoxy]-11'-(tert-butyldimethylsiloxy)dodecahydro-10'-hydroxy-2'-[(p-methoxybenzyl)oxy]-6'-(methoxymethoxy)-2,2,4'a,13',13'-pentamethylspiro(1,3-dioxolane-4,1'(5'H)-[7,10]methanobenzocyclodec...) (171625-80-2) → (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.04,9]pentadecan-3-one (251950-67-1)

Guidance literature:

With water; acetic acid;

DOI:10.1055/s-1999-2911

Reference yield: 94.0%

benzoic acid anhydride (93-97-0) + (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.04,9]pentadecan-3-one (251950-67-1) → C58H64O14 (251950-70-6)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1055/s-1999-2911

Reference yield: 82.0%

benzoic acid anhydride (93-97-0) + (1S,2R,4S,5S,7R,8S,9S,11S,12S)-5-Benzyloxymethoxy-8,11,12-trihydroxy-8-hydroxymethyl-7-(4-methoxy-benzyloxy)-2-methoxymethoxy-4,15,15-trimethyl-tricyclo[10.2.1.04,9]pentadecan-3-one (251950-67-1) → C51H60O13

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1055/s-1999-2911

upstream raw materials:

(2'R,4S,4'S,4'aS,6'R,7'S,10'S,11'S,12'aS)-4'-[(Benzyloxy)methoxy]-11'-(tert-butyldimethylsiloxy)dodecahydro-10'-hydroxy-2'-[(p-methoxybenzyl)oxy]-6'-(methoxymethoxy)-2,2,4'a,13',13'-pentamethylspiro(1,3-dioxolane-4,1'(5'H)-[7,10]methanobenzocyclodec...)

Downstream raw materials:

C₅₈H₆₄O₁₄

C₄₉H₆₆O₁₃Si

C₅₆H₇₀O₁₄Si

C₆₄H₇₈O₁₅Si

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