4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

Base Information

Chemical Name:4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid
CAS No.:1323432-95-6
Molecular Formula:C₁₀H₁₂O₂
Molecular Weight:174.094
Hs Code.:

4-(phenyl-<SUP>13</SUP>C<SUB>6</SUB>)butanoic-1,2,3,4-<SUP>13</SUP>C<SUB>4</SUB> acid

Synonyms:4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

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Chemical Property of 4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

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Technology Process of 4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

There total 2 articles about 4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1323432-93-4,1346600-75-6
4-oxo-4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

: 1323432-95-6
4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

Guidance literature:: 4-oxo-4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid; With hydrazine hydrate; In diethylene glycol; at 20 ℃; for 0.5h;

With potassium hydroxide; In diethylene glycol; at 120 - 215 ℃;
DOI:10.1039/c0ob01107j

Reference yield:

: 32488-44-1
benzene-⁽¹³⁾C₆

: 1323432-95-6
4-(phenyl-¹³C₆)butanoic-1,2,3,4-¹³C₄ acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / 1,1,2,2-tetrachloroethane

2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C

2.2: 120 - 215 °C

With aluminum (III) chloride; hydrazine hydrate; In 1,1,2,2-tetrachloroethane; diethylene glycol; 2.1: Wolff-Kishner reduction / 2.2: Wolff-Kishner reduction;
DOI:10.1039/c0ob01107j