2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

Base Information

Chemical Name:2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine
CAS No.:173850-06-1
Molecular Formula:C₁₈H₂₂N₄O₄S
Molecular Weight:390.463
Hs Code.:

Synonyms:2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

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Chemical Property of 2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

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Technology Process of 2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

There total 4 articles about 2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 173850-04-9
2-(pivaloylamino)-4(3H)-oxo-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

: 173850-06-1
2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; for 5h; under 760 Torr;
DOI:10.1021/jo951471k

Reference yield:

: 137281-08-4
N-(4-oxo-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl)pivalamide

: 173850-06-1
2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temperature

2: 94 percent / H₂ / Pd(OH)2/C / methanol / 5 h / 760 Torr

With hydrogen; sodium hydride; palladium dihydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo951471k

Reference yield:

: 173850-03-8
2-(pivaloylamino)-4(3H)-oxo-7-acetyl-7H-pyrrolo<2,3-d>pyrimidine

: 173850-06-1
2-(pivaloylamino)-4(3H)-oxo-5,6-dihydro-7-tosyl-7H-pyrrolo<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / H₂ / PtO₂ / acetic acid; methanol / 12 h / 2585.7 Torr

2: 71 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temperature

3: 94 percent / H₂ / Pd(OH)2/C / methanol / 5 h / 760 Torr

With hydrogen; sodium hydride; platinum(IV) oxide; palladium dihydroxide; In methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo951471k