3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

Base Information

Chemical Name:3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane
CAS No.:30116-14-4
Molecular Formula:C₃₉H₃₉N₃O₆S₃
Molecular Weight:741.953
Hs Code.:

Synonyms:3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

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Chemical Property of 3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

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Technology Process of 3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

There total 9 articles about 3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 18522-92-4
sodium p-toluenesulfonamide

: 223450-27-9
7,15-Bis-bromomethyl-3,11-bis-(toluene-4-sulfonyl)-3,11-diaza-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene

: 30116-14-4
3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1055/s-1999-3385

Reference yield:

: 18303-10-1
benzyl N-(4-methylbenzenesulfonyl)carbamate

: 30116-14-4
3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / K₂CO₃ / dimethylformamide / 72 h

2: 61 percent / K₂CO₃ / dimethylformamide / 72 h / 20 °C

3: 80 percent / LiBH₄ / tetrahydrofuran / 24 h / Heating

4: 82 percent / PBr₃ / CHCl₃ / 48 h / Heating

5: 70 percent / Cs₂CO₃ / dimethylformamide / 24 h / 90 °C

With lithium borohydride; phosphorus tribromide; potassium carbonate; caesium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3385

Reference yield:

: 29333-41-3
methyl 3,5-bis(bromomethyl)benzoate

: 30116-14-4
3,7,10-tris-(toluene-4-sulfonyl)-3,7,10-triaza-1,5(1,3,5)-dibenzena-bicyclo[3.3.3]undecaphane

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / K₂CO₃ / dimethylformamide / 72 h

2: 61 percent / K₂CO₃ / dimethylformamide / 72 h / 20 °C

3: 80 percent / LiBH₄ / tetrahydrofuran / 24 h / Heating

4: 82 percent / PBr₃ / CHCl₃ / 48 h / Heating

5: 70 percent / Cs₂CO₃ / dimethylformamide / 24 h / 90 °C

With lithium borohydride; phosphorus tribromide; potassium carbonate; caesium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3385