C₁₀H₁₁Cl₂N₂PS

Base Information

• Chemical Name: C₁₀H₁₁Cl₂N₂PS
• CAS No.: 138404-32-7
• Molecular Formula: C₁₀H₁₁Cl₂N₂PS
• Molecular Weight: 293.157

Synonyms:C₁₀H₁₁Cl₂N₂PS

Chemical Property of C₁₀H₁₁Cl₂N₂PS

Chemical Property:

Purity/Quality:

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Technology Process of C₁₀H₁₁Cl₂N₂PS

There total 2 articles about C₁₀H₁₁Cl₂N₂PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-Amino-3-benzyl-4,5-dihydro-thiazol-3-ium; bromide → C10H11Cl2N2PS (138404-32-7)

Guidance literature:

With triethylamine; phosphorus trichloride; In toluene; Ambient temperature;

DOI:10.1016/0040-4039(91)80188-C

Reference yield:

benzyl bromide (100-39-0) → C10H11Cl2N2PS (138404-32-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / tetrahydrofuran / 20 °C

2: PCl₃; Et₃N / CH₂Cl₂ / 0 - 20 °C

With triethylamine; phosphorus trichloride; In tetrahydrofuran; dichloromethane;

DOI:10.1080/10426500307803

Reference yield:

C10H11Cl2N2PS (138404-32-7) + ortho-cresol (95-48-7,77504-84-8) → C17H18ClN2OPS2 + (3-benzyl-thiazolidin-2-ylidene)-thiophosphoramidic acid O,O'-di-o-tolyl ester

Guidance literature:

With sulfur; triethylamine; In dichloromethane; at 20 ℃; Title compound not separated from byproducts;

DOI:10.1080/10426500307803

upstream raw materials:

benzyl bromide

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